反应条件
1: 7-Bromo-1H-indole With sodium hydride in N,N-dimethyl-formamide; mineral oil T=0°C; 1 h; Inert atmosphere; 2: p-toluenesulfonyl chloride in N,N-dimethyl-formamide; mineral oil 0.333333 h; Inert atmosphere;
参考文献
AMGEN INC.; ASHTON, Kate; BARTBERGER, Michael D.; BOURBEAU, Matthew Paul; CROGHAN, Michael D.; FOTSCH, Christopher H.; HUNGATE, Randall W.; KONG, Ke; NISHIMURA, Nobuko; NORMAN, Mark H.; PENNINGTON, Lewis D.; REICHELT, Andreas; SIEGMUND, Aaron C.; TADESSE, Seifu; ST. JEAN, David Jr; YANG, Kevin C.; YAO, Guomin
Patent: WO2013/173382 A1, 2013 ;
Location in patent: Page/Page column 206-207 ;