反应条件
1: 96 percent / K2CO3 / 0.5 h / Ambient temperature
2: 98 percent / HCl / methanol; H2O / 30 h
3: 1.) 4-NO2-C6H6-SO2-N3, 1,4-diazabicyclo<2.2.2>octan, 2.) tBuOCl, HCOOH, ascorbinic acid / 1.) DMF, 0 deg C, 2.) H2O, r.t., 1 h
View Scheme
参考文献
Gleiter, Rolf; Dobler, Walter
Chemische Berichte, 1985 , vol. 118, # 12 p. 4725 - 4742
