反应条件
1: 95 percent / NCS, DMS / CH2Cl2 / -40 - 0 °C
2: tetrahydrofuran / -78 °C
3: 82 percent / TBAF / tetrahydrofuran / 1.) 0 deg C, 1 h, 2.) room temperature, 3 h
View Scheme
参考文献
Sen, Stephanie E.; Ewing, Gregory J.
Journal of Organic Chemistry, 1997 , vol. 62, # 11 p. 3529 - 3536
