反应条件
1: Dess-Martin periodinane / CH2Cl2 / 1 h / 20 °C 2: 0.052 g / NaBH4 / methanol; tetrahydrofuran / 1 h / -78 - 20 °C 3: 94 percent / hydrogen fluoride-pyridine; pyridine / tetrahydrofuran / 2 h / 20 °C 4: 92 percent / HF*pyridine / tetrahydrofuran / 2 h / 0 - 20 °C 5: 97 percent / 3,3-dimethyldioxirane / CH2Cl2; acetone / 2.5 h / -78 - -50 °C View Scheme
参考文献
Su, Dai-Shi; Meng, Dongfang; Bertinato, Peter; Balog, Aaron; Sorensen, Erik J.; Danishefsky, Samuel J.; Zheng, Yu-Huang; Chou, Ting-Chao; He, Lifeng; Horwitz, Susan B.
Angewandte Chemie (International Edition in English), 1997 , vol. 36, # 7 p. 757 - 759
