sulfuryl dichloride in acetic acid T=60°C; 0.5 h; Inert atmosphere;
参考文献
Shiraki, Hiroaki; Kozar, Michael P.; Melendez, Victor; Hudson, Thomas H.; Ohrt, Colin; Magill, Alan J.; Lin, Ai J.
Journal of Medicinal Chemistry, 2011 , vol. 54, # 1 p. 131 - 142
1.1: sulfuryl dichloride / acetic acid / 0.5 h / 60 °C / Inert atmosphere 2.1: phosphorous pentoxide / diethylphosphoric acid ethyl ester / 1 h / 20 °C / Inert atmosphere 2.2: 0.25 h / 35 °C / Reflux; Inert atmosphere View Scheme
参考文献
Shiraki, Hiroaki; Kozar, Michael P.; Melendez, Victor; Hudson, Thomas H.; Ohrt, Colin; Magill, Alan J.; Lin, Ai J.
Journal of Medicinal Chemistry, 2011 , vol. 54, # 1 p. 131 - 142
