3-氨基-2-甲基-4(3H)喹唑啉酮合成路线 （共 61 条）
反应条件
1: 80 percent / gl. acetic acid / ethanol / 5 h / Heating 2: 1) aq. NaNO2, gl. acetic acid, HCl / 1) 0-5 deg C, 2) pyridine, r.t., overnight View Scheme
参考文献
Singh, Shradha; Shukla, Mukundja; Srivastava, Vijai K.; Shanker, K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 368 - 370
反应条件
1: With n-butyllithium in tetrahydrofuran T=-78°C; 0.75 h; 2: With carbon monoxide in tetrahydrofuran T=0°C; 2 h;
参考文献
Arques, A.; Molina, P.; Soler, A.
Synthesis, 1980 , # 9 p. 702 - 704
反应条件
lead(IV) acetate; 1-hexene in dichloromethane 0.25 h; Ambient temperature;
参考文献
Atkinson, Robert S.; Malpass, John R.; Skinner, Karen L.; Woodthorpe, Katherine L.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 8 p. 1905 - 1912
反应条件
lead(IV) acetate in dichloromethane 0.25 h; Ambient temperature;
参考文献
Atkinson, Robert S.; Malpass, John R.; Skinner, Karen L.; Woodthorpe, Katherine L.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 8 p. 1905 - 1912
参考文献
Bogert; Gortner
Journal of the American Chemical Society, 1909 , vol. 31, p. 944
反应条件
in ethanol T=70 - 80°C; 0.333333 h;
参考文献
Arques, A.; Molina, P.; Soler, A.
Synthesis, 1980 , # 9 p. 702 - 704
反应条件
pyridine in benzene 2 h; Heating;
参考文献
Ibrahim, S. S.; Abdel-Halim, A. M.; Gabr, Y.; El-Edfawy, S.; Abdel-Rahman, R. M.
Journal of Chemical Research, Miniprint, 1997 , # 5 p. 1041 - 1063
反应条件
pyridine in benzene
2 h; Heating;
参考文献
Ibrahim, S. S.; Abdel-Halim, A. M.; Gabr, Y.; El-Edfawy, S.; Abdel-Rahman, R. M.
Journal of Chemical Research, Miniprint, 1997 , # 5 p. 1041 - 1063
反应条件
24 h; Ambient temperature;
参考文献
Merour
Journal of Heterocyclic Chemistry, 1982 , vol. 19, # 6 p. 1425 - 1431
参考文献
Tyagi, Mirdula; Srivastava; Chandra, Ramesh; Kumar, Ashok
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2002 , vol. 41, # 11 p. 2367 - 2370
