二苯并[B,F]硫杂卓-10(11H)-酮合成路线 （共 4 条）
反应条件
1: NaBH4 / methanol / 0.33 h / 0 °C 2: SOCl2 / 0.17 h / Ambient temperature View Scheme
参考文献
Kurokawa; Sato; Masuda; Yoshida; Ochi; Zushi; Fujiwara; Naruto; Uno; Matsumoto
Chemical and Pharmaceutical Bulletin, 1991 , vol. 39, # 10 p. 2564 - 2573
反应条件
1: 1.) ZnI2, 2.) POCl3 / 1.) benzene, R.T. 8 h, 2.) pyridine, reflux 6 h.
2: 38 percent / NaBH4, 20 percent NaOH / ethanol / 11 h / Heating
View Scheme
参考文献
Sindelar; Holubek; Ryska; et al.
Collection of Czechoslovak Chemical Communications, 1983 , vol. 48, # 4 p. 1187 - 1211
反应条件
1: 1.) ZnI2, 2.) POCl3 / 1.) benzene, R.T. 8 h, 2.) pyridine, reflux 6 h.
2: 1.) NaBH4, 20 percent NaOH, KOH / 1.) ethanol, reflux 11 h, 2.) reflux 5 h.
View Scheme
参考文献
Sindelar; Holubek; Ryska; et al.
Collection of Czechoslovak Chemical Communications, 1983 , vol. 48, # 4 p. 1187 - 1211
反应条件
1: selenium(IV) oxide; acetic acid
2: ammonium acetate; acetic acid
View Scheme
参考文献
Pesic, Dijana; Landek, Ivana Ozimec; Rupcic, Renata; Modric, Marina; Dzapo, Iva; Trojko, Rudolf; Mercep, Mladen; Mesic, Milan
Journal of Heterocyclic Chemistry, 2012 , vol. 49, # 2 p. 243 - 252
