反应条件
1.1: sodium hydride / mineral oil; tetrahydrofuran / 1 h / 0 °C / |Inert atmosphere 1.2: 1.75 h / 0 - 20 °C / |Inert atmosphere 2.1: n-butyllithium / diethyl ether; hexane / 1 h / -65 °C / |Inert atmosphere 2.2: 1 h / -65 °C / |Inert atmosphere 3.1: hydrogenchloride / diethyl ether; hexane; water / |Inert atmosphere View Scheme
参考文献
Adamczyk-Wozniak, Agnieszka; Brzozka, Zbigniew; Dabrowski, Marek; Madura, Izabela D.; Scheidsbach, Roy; Tomecka, Ewelina; Zukowski, Kamil; Sporzynski, Andrzej
Journal of Molecular Structure, 2013 , vol. 1035, p. 190 - 197