二-μ-氯代双[2-[(二甲基氨基)甲基]-4,6-二甲氧基苯基-C,N]二钯(II)合成路线 (共 1 条)
反应条件
in methanol soln. of benzylamine in MeOH treated with soln. of Li2PdCl4 in MeOH, kept for 24 h at 24-33 °C; ppt. sepd., washed with MeOH, dried at room temp., dissolved in hot CHCl3, filtered through column of Celite, filtrate crystd. from CHCl3 or CHCl3/MeOH; elem. anal.;
参考文献
Barr, Neal; Dyke, Stanley F.
Journal of Organometallic Chemistry, 1983 , vol. 243, # 2 p. 223 - 232