甲基10-氧代十一烷酸酯合成路线 （共 18 条）
反应条件
oxygen; copper(l) chloride; palladium dichloride in tetrahydrofuran; water
T=20°C; 10 h;
参考文献
Dzhemileva, G. A.; Odinokov, V. N.; Dzhemilev, U. M.; Tolstikov, G. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 2 p. 307 - 312
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 2 p. 343 - 348
反应条件
bis(benzonitrile)palladium(II) dichloride; AgNO2; CuCl2·2H2O; nitromethane; oxygen; tert-butyl alcohol
T=20°C; Wacker Oxidation; P=760.051 Torr; 6 h; Overall yield = 72 percent;
参考文献
Wickens, Zachary K.; Morandi, Bill; Grubbs, Robert H.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 43 p. 11257 - 11260
Angew. Chem., 2013 , vol. 125, # 43 p. 11467 - 11470
反应条件
pyridine; Ag2CrO4; water; iodine in dichloromethane
1.) 20 min, 0 deg C, 2.) 1 h, room temperature or without water;
参考文献
Khan, Mushfiquddin; Agarwal, Rajiv; Ahmad, Suhail; Ahmad, F.; Osman, S. M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1988 , vol. 27, # 1-12 p. 430 - 434
反应条件
[Co(PPh3)3Cl] in benzene
T=60°C; 7.5 h;
参考文献
Momose, Den-ichi; Iguchi, Kazuo; Sugiyama, Toshikazu; Yamada, Yasuji
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 5 p. 1840 - 1853
反应条件
silver hexafluoroantimonate; water
T=75°C; 48 h; chemoselective reaction;
参考文献
Thuong, Mathieu Bui The; Mann, Andre; Wagner, Alain
Chemical Communications, 2012 , vol. 48, # 3 p. 434 - 436
反应条件
[Co(PPh3)3Cl] in benzene
T=60°C; 7.5 h; Yield given;
参考文献
Momose, Den-ichi; Iguchi, Kazuo; Sugiyama, Toshikazu; Yamada, Yasuji
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 5 p. 1840 - 1853
反应条件
[Co(PPh3)3Cl]; triethylamine in benzene
6 h; Ambient temperature;
参考文献
Momose, Den-ichi; Iguchi, Kazuo; Sugiyama, Toshikazu; Yamada, Yasuji
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 5 p. 1840 - 1853
反应条件
CuCN in tetrahydrofuran
参考文献
Whitman, David B.; Askew, Ben C.; Duong, Le T.; Fernandez-Metzler, Carmen; Halczenko, Wasyl; Hartman, George D.; Hutchinson, John H.; Leu, Chih-Tai; Prueksaritanont, Thomayant; Rodan, Gideon A.; Rodan, Sevgi B.; Duggan, Mark E.
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 17 p. 4411 - 4415
反应条件
[Co(PPh3)3Cl]
6 h; Ambient temperature; Yield given. Further byproducts given;
参考文献
Momose, Den-ichi; Yamada, Yasuji
Tetrahedron Letters, 1983 , vol. 24, # 26 p. 2669 - 2672
反应条件
pyridine; Ag2CrO4; iodine in dichloromethane
1.) 20 min, 0 deg C, 2.) 1 h, room temperature;
参考文献
Khan, Mushfiquddin; Agarwal, Rajiv; Ahmad, Suhail; Ahmad, F.; Osman, S. M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1988 , vol. 27, # 1-12 p. 430 - 434
