M-(二乙基氨基)苯基乙酸酯合成路线 (共 3 条)
反应条件
sodium hydroxide 2 h;
参考文献
Pirrung; Fallon; Zhu; Yong Rok Lee
Journal of the American Chemical Society, 2001 , vol. 123, # 16 p. 3638 - 3643
反应条件
1: diethyl ether / 3 h / Heating 2: 2 M aq. NaOH / tetrahydrofuran / 20 °C View Scheme
参考文献
Corrie; Munasinghe; Rettig
Journal of Heterocyclic Chemistry, 2000 , vol. 37, # 6 p. 1447 - 1455
反应条件
1: diethyl ether / 3 h / Heating 2: 2 M aq. NaOH / tetrahydrofuran / 20 °C 3: 75 percent / Et3N; PhOPOCl2 / 1,2-dichloro-ethane / 3.5 h / Heating 4: 63 percent / 0.5 M aq. NaOH / ethanol / 3 h / 20 °C View Scheme
参考文献
Corrie; Munasinghe; Rettig
Journal of Heterocyclic Chemistry, 2000 , vol. 37, # 6 p. 1447 - 1455