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63148-62-9
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
189999-35-7
合成路线
（共 17 条）
189999-35-7
+
74497-02-2
→
反应条件
1150-62-5
9-苯基咔唑
+
2113-51-1
2-碘联苯
反应条件
palladium diacetate; caesium carbonate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in para-xylene T=125°C; 2.5 h; Inert atmosphere;
参考文献
Beilstein Journal of Organic Chemistry, , vol. 9, p. 1202 - 1209
189999-35-7
+
100-46-9
苄胺
→
反应条件
19402-87-0
9-苄基咔唑
反应条件
palladium diacetate; caesium carbonate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in para-xylene T=125°C; 3 h; Inert atmosphere;
参考文献
Riedmueller, Stefan; Nachtsheim, Boris J.
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 1202 - 1209
189999-35-7
+
109-73-9
正丁胺
→
反应条件
1484-08-8
N-正丁基咔唑
反应条件
copper(l) iodide; copper diacetate; sodium carbonate; ethylene glycol in isopropyl alcohol T=85°C; Ullmann Condensation; 16 h; Inert atmosphere;
参考文献
Zhu, Daqian; Liu, Qi; Luo, Bingling; Chen, Meihui; Pi, Rongbiao; Huang, Peng; Wen, Shijun
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 11-12 p. 2172 - 2178
189999-35-7
+
5720-05-8
4-甲基苯硼酸
+
766-97-2
4-甲苯基乙炔
→
反应条件
80077-84-5
反应条件
copper(l) iodide; palladium diacetate; sodium carbonate; triphenylphosphine in N,N-dimethyl-formamide T=100°C; 12 h; Inert atmosphere;
参考文献
Zhu, Daqian; Wu, Yongcheng; Wu, Baojian; Luo, Bingling; Ganesan; Wu, Fu-Hai; Pi, Rongbiao; Huang, Peng; Wen, Shijun
Organic Letters, 2014 , vol. 16, # 9 p. 2350 - 2353
189999-35-7
+
766-97-2
4-甲苯基乙炔
→
反应条件
80077-84-5
反应条件
1: palladium diacetate; copper(l) iodide; triphenylphosphine; sodium carbonate / N,N-dimethyl-formamide / 12 h / 100 °C / |Inert atmosphere 2: palladium diacetate; copper(l) iodide; triphenylphosphine; sodium carbonate / N,N-dimethyl-formamide / 12 h / 100 °C / |Inert atmosphere View Scheme
参考文献
Zhu, Daqian; Wu, Yongcheng; Wu, Baojian; Luo, Bingling; Ganesan; Wu, Fu-Hai; Pi, Rongbiao; Huang, Peng; Wen, Shijun
Organic Letters, 2014 , vol. 16, # 9 p. 2350 - 2353
189999-35-7
+
873-74-5
对氨基苯腈
→
反应条件
57103-17-0
反应条件
palladium diacetate; caesium carbonate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in para-xylene T=125°C; 3 h; Inert atmosphere;
参考文献
Riedmueller, Stefan; Nachtsheim, Boris J.
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 1202 - 1209
189999-35-7
+
92-67-1
4-氨基联苯
→
反应条件
6299-16-7
9-(4-苯基苯基)咔唑
反应条件
palladium diacetate; caesium carbonate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in para-xylene T=125°C; 3 h; Inert atmosphere;
参考文献
Riedmueller, Stefan; Nachtsheim, Boris J.
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 1202 - 1209
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