反应条件
1: 1.) sodium hydride / 1.) THF, RT, 30 min, 2.) THF, RT, 1 h 2: 1.) n-butyllithium / 1.) ether, hexane, RT, 2h, 2.) hexane, ether, RT, overnight 3: 17 percent / HCl / acetone / 3 h / Ambient temperature View Scheme
参考文献
Synthetic Communications, , vol. 24, # 7 p. 1009 - 1018