2-乙基-3-甲基-1H-吲哚合成路线 (共 40 条)
反应条件
1,3-bis(3-sulfopropyl)-1H-imidazol-3-ium trifluoromethanesulfonate in water
T=100°C; Fischer Indole Synthesis; 0.25 h; Microwave irradiationGreen chemistry;
参考文献
Li, Bai Lin; Zhong, Ai Guo; Xu, Dan-Qian
Journal of Fluorine Chemistry, 2012 , vol. 144, p. 45 - 50,6
反应条件
potassium hydrogensulfate; silica gel in acetonitrile
T=20°C; 7 h;
参考文献
Kapoor, Kamal K.; Ganai, Bilal A.; Kumar, Satish; Andotra, Charanjeet S.
Synthetic Communications, 2006 , vol. 36, # 18 p. 2727 - 2735
反应条件
[S-BINAP]PdBr2; hydrogen in dichloromethane
T=120°C; P=41372.9 Torr; 24 h; Autoclave;
参考文献
Cabrera; Sharma; Ayala; Rubio-Perez; Amezquita-Valencia, Manuel
Tetrahedron Letters, 2011 , vol. 52, # 50 p. 6758 - 6762
反应条件
zinc trifluoromethanesulfonate in toluene
T=100°C; 8 h;
参考文献
Kumar, Manyam Praveen; Liu, Rai-Shung
Journal of Organic Chemistry, 2006 , vol. 71, # 13 p. 4951 - 4955
反应条件
FeBr2 in toluene
T=140°C; 16 h; Schlenk techniqueInert atmosphere;
参考文献
Nguyen, Quyen; Nguyen, Tuyen; Driver, Tom G.
Journal of the American Chemical Society, 2013 , vol. 135, # 2 p. 620 - 623
反应条件
[(IPr)Pd(acac)Cl]; potassium tert-butylate; magnesium sulfate in toluene
T=100°C; 12 h; Inert atmosphere;
参考文献
Jin, Zhong; Guo, Su-Xian; Qiu, Ling-Ling; Wu, Gui-Ping; Fang, Jian-Xin
Applied Organometallic Chemistry, 2011 , vol. 25, # 7 p. 502 - 507
反应条件
[(IPr)Pd(acac)Cl]; potassium tert-butylate; magnesium sulfate in toluene
T=100°C; 12 h; Inert atmosphere;
参考文献
Jin, Zhong; Guo, Su-Xian; Qiu, Ling-Ling; Wu, Gui-Ping; Fang, Jian-Xin
Applied Organometallic Chemistry, 2011 , vol. 25, # 7 p. 502 - 507
反应条件
phosphorus trichoride in benzene
Ambient temperature;
参考文献
Baccolini, Graziano; Todesco, Paolo E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 3 p. 535 - 538
反应条件
sodium acetate; iron; acetic acid in ethanol; water
2 h; Heating;
参考文献
Raucher, Stanley; Koolpe, Gary A.
Journal of Organic Chemistry, 1983 , vol. 48, # 12 p. 2066 - 2069
反应条件
RuCl3*xH2O; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene
T=110 - 170°C; 25 h;
参考文献
Tursky, Matyas; Lorentz-Petersen, Linda L. R.; Olsen, Lasse B.; Madsen, Robert
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 24 p. 5576 - 5582