2-甲氧基-5-(2-噻吩)苯甲醛合成路线 (共 2 条)
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in ethylene glycol dimethyl ether; water Suzuki Coupling; 2.16667 h; Heating / reflux;
参考文献
ATHEROGENICS, INC.
Patent: WO2006/4903 A2, 2006 ;
Location in patent: Page/Page column 79-80 ;
反应条件
1: thiophene With potassium permanganate; acetic acid Microwave irradiation; 2: (3-formyl-4-methoxyphenyl)boronic acid 0.5 h; Microwave irradiation;
参考文献
Demir, Ayhan S.; Findik, Hamide; Saygili, Nezire; Tuna Subasi
Tetrahedron, 2010 , vol. 66, # 6 p. 1308 - 1312