4-吡啶甲酰胺,N,N-二甲基-合成路线 （共 6 条）
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in trichloroethane, 1,1,2-; water T=90°C; 24 h;
参考文献
Liu, Zhaojun; Zhang, Jie; Chen, Shulin; Shi, Erbo; Xu, Yuan; Wan, Xiaobing
Angewandte Chemie - International Edition, 2012 , vol. 51, # 13 p. 3231 - 3235
参考文献
Meltzer et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 4062,4064
反应条件
thionyl chloride T=150°C; 5 h; Inert atmosphere;
参考文献
Kumagai, Takashi; Anki, Tomohiro; Ebi, Takahiro; Konishi, Akihito; Matsumoto, Kouzou; Kurata, Hiroyuki; Kubo, Takashi; Katsumoto, Kenta; Kitamura, Chitoshi; Kawase, Takeshi
Tetrahedron, 2010 , vol. 66, # 46 p. 8968 - 8973
反应条件
phosphorus pentoxide; toluene
参考文献
Swain; Naegele
Journal of the American Chemical Society, 1957 , vol. 79, p. 5250,5252
反应条件
in diethyl ether
1 h; Ambient temperature;
参考文献
Epsztajn, Jan; Berski, Zbigniew; Brzezinski, Jacek Z.; Jozwiak, Andrzej
Tetrahedron Letters, 1980 , vol. 21, p. 4739 - 4742
反应条件
trichlorophosphate in toluene
4 h; Heating;
参考文献
Arbuzov, B. A.; Aganov, A. V.; Zobova, N. N.; Klochkov, V. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 4 p. 544 - 548
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 4 p. 758 - 762
