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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
190380-40-6
合成路线
（共 4 条）
190380-35-9
→
反应条件
190380-40-6
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane 24 h; Heating;
参考文献
Bebot, Monique; Coudert, Pascal; Rubat, Catherine; Vallee-Goyet, Danielle; Gardette, Daniel; Mavel, Sylvie; Albuisson, Eliane; Couquelet, Jacques
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 4 p. 659 - 667
89-98-5
2-氯苯甲醛
→
反应条件
190380-40-6
反应条件
1: HCl 2: 48 percent / hydroxylamine hydrochloride, pyridine / 10 h / Heating 3: 20 percent / N-bromosuccinimide, 2,2'-azobisisobutyronitrile / CCl4 / 24 h / Heating View Scheme
参考文献
Bebot, Monique; Coudert, Pascal; Rubat, Catherine; Vallee-Goyet, Danielle; Gardette, Daniel; Mavel, Sylvie; Albuisson, Eliane; Couquelet, Jacques
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 4 p. 659 - 667
123-76-2
乙酰丙酸
→
反应条件
190380-40-6
反应条件
1: HCl 2: 48 percent / hydroxylamine hydrochloride, pyridine / 10 h / Heating 3: 20 percent / N-bromosuccinimide, 2,2'-azobisisobutyronitrile / CCl4 / 24 h / Heating View Scheme
参考文献
Bebot, Monique; Coudert, Pascal; Rubat, Catherine; Vallee-Goyet, Danielle; Gardette, Daniel; Mavel, Sylvie; Albuisson, Eliane; Couquelet, Jacques
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 4 p. 659 - 667
132372-47-5
→
反应条件
190380-40-6
反应条件
1: 48 percent / hydroxylamine hydrochloride, pyridine / 10 h / Heating 2: 20 percent / N-bromosuccinimide, 2,2'-azobisisobutyronitrile / CCl4 / 24 h / Heating View Scheme
参考文献
Bebot, Monique; Coudert, Pascal; Rubat, Catherine; Vallee-Goyet, Danielle; Gardette, Daniel; Mavel, Sylvie; Albuisson, Eliane; Couquelet, Jacques
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 4 p. 659 - 667
