(S)-γ-Valerolactone合成路线 （共 69 条）
反应条件
hydrogenchloride; hydrogen; RuCl2-(S)-BINAP*Et3N in ethanol T=50°C; Noyori hydrogenation; P=72400.7 Torr; 120 h;
参考文献
Stangeland, Eric L.; Sammakia, Tarek
Journal of Organic Chemistry, 2004 , vol. 69, # 7 p. 2381 - 2385
反应条件
hydrogen; Ru(OCOCH3)2((R)-2,2'-bis(diphenylphosphino)-1,1'-binaphthyl) in dichloromethane T=50°C; P=76000 Torr; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 60, # 2 p. 357 - 363
反应条件
Raney-Ni (W6) in methanol 6 h; Heating;
参考文献
White, James D.; Somers, Todd C.; Reddy, G. Nagabushana
Journal of the American Chemical Society, 1986 , vol. 108, # 17 p. 5352 - 5353
反应条件
hydrogen; potassium hydrogencarbonate; palladium on activated charcoal in ethyl acetate P=1900 Torr;
参考文献
Ortuno, Rosa M.; Alonso, Daniel; Cardellach, Jaume; Font, Josep
Tetrahedron, 1987 , vol. 43, # 9 p. 2191 - 2198
反应条件
2,6-dimethylpyridine; sodium perchlorate in acetonitrile Electrolysis;
参考文献
Kashiwagi, Yoshitomo; Kurashima, Futoshi; Chiba, Shinya; Anzai, Jun-Ichi; Osa, Tetsuo; Bobbitt, James M.
Chemical Communications, 2003 , # 1 p. 114 - 115
反应条件
trifluoroacetic acid in dichloromethane
参考文献
Manzocchi, Ada; Casati, Rosangela; Fiecchi, Alberto; Santaniello, Enzo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 2753 - 2758
反应条件
hydrogenchloride; hydrogen; (S)-(-)-2,2'-bis(diphenylphosphino)-1,1'-binaphthyl; [Ru(η4-COD)(η3-methylallyl)2] in methanol; ethanol T=60°C; P=45600 - 53200 Torr; 5 h;
参考文献
Russian Chemical Bulletin, , vol. 54, # 10 p. 2374 - 2378
反应条件
hydrogenchloride in water T=95°C; 8 h;
参考文献
Tsuboi, Sadao; Sakamoto, Jun-ichi; Kawano, Takayuki; Utaka, Masanori; Takeda, Akira
Journal of Organic Chemistry, 1991 , vol. 56, # 25 p. 7177 - 7179
反应条件
hydrogenchloride; hydrogen; (S)-(-)-2,2'-bis(diphenylphosphino)-1,1'-binaphthyl; [Ru(η4-COD)(η3-methylallyl)2] in methanol; ethanol T=60°C; P=45600 - 53200 Torr; 5 h;
参考文献
Russian Chemical Bulletin, , vol. 54, # 10 p. 2374 - 2378
反应条件
hydrogenchloride; poly(diallyldimethylammonium) hexafluorophosphate; hydrogen; (S)-(-)-2,2'-bis(diphenylphosphino)-1,1'-binaphthyl; [Ru(η4-COD)(η3-methylallyl)2] in methanol T=60°C; P=45600 Torr; 3 h;
参考文献
Mendeleev Communications, , vol. 17, # 1 p. 20 - 21
