(4-氯苯基)甲基4-氯苯甲酸酯合成路线 （共 17 条）
反应条件
diethyl allyl phosphate; potassium carbonate; palladium diacetate in N,N-dimethyl-formamide
4 h;
参考文献
Shvo, Youval; Goldman-Lev, Vered
Journal of Organometallic Chemistry, 2002 , vol. 650, # 1-2 p. 151 - 156
反应条件
4-tert-butylbenzyl mercaptan; Di-n-butylmagnesium in tetrahydrofuran
T=65°C; Tishchenko-Claisen Dismutation;
参考文献
Curran, Simon P.; Connon, Stephen J.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 43 p. 10866 - 10870
The Thiolate-Catalyzed Intermolecular Crossed Tishchenko Reaction: Highly Chemoselective Coupling of Two Different Aromatic Aldehydes, 2012 , vol. 124, # 43 p. 11024 - 11028,5
参考文献
Rueggeberg; Ginsburg; Frantz
Journal of the American Chemical Society, 1945 , vol. 67, p. 2154
反应条件
1: potassium hydroxide; [bis(acetoxy)iodo]benzene / 3 h / 0 °C
2: toluene-4-sulfonic acid / tetrahydrofuran; water / 4.5 h / |Reflux
3: potassium carbonate; 18-crown-6 ether; oxygen / tetrahydrofuran; water / 24 h / 70 °C / 760.05 Torr
View Scheme
参考文献
Liu, Hui; Dong, Chao; Zhang, Zeguang; Wu, Peiyu; Jiang, Xuefeng
Angewandte Chemie - International Edition, 2012 , vol. 51, # 50 p. 12570 - 12574
Angew. Chem., 2012 , vol. 124, # 50 p. 12738 - 12742,5
反应条件
1: toluene-4-sulfonic acid / tetrahydrofuran; water / 4.5 h / |Reflux
2: potassium carbonate; 18-crown-6 ether; oxygen / tetrahydrofuran; water / 24 h / 70 °C / 760.05 Torr
View Scheme
参考文献
Liu, Hui; Dong, Chao; Zhang, Zeguang; Wu, Peiyu; Jiang, Xuefeng
Angewandte Chemie - International Edition, 2012 , vol. 51, # 50 p. 12570 - 12574
Angew. Chem., 2012 , vol. 124, # 50 p. 12738 - 12742,5
反应条件
1: thionyl chloride; pyridine / dichloromethane
2: dimethylsulfoxide-d6 / 35 °C / |Irradiation
View Scheme
参考文献
Grenga, Paolo N.; Stoutenburg, Eric G.; Priefer, Ronny
Tetrahedron Letters, 2012 , vol. 53, # 37 p. 4933 - 4937
反应条件
in dimethylsulfoxide-d6
T=35°C; Irradiation; Solvent;
参考文献
Grenga, Paolo N.; Stoutenburg, Eric G.; Priefer, Ronny
Tetrahedron Letters, 2012 , vol. 53, # 37 p. 4933 - 4937
