3-氯-1-(10,11-二氢-5H-二苯并[b,f]氮杂卓-5-基)-1-丙酮合成路线 （共 6 条）
反应条件
in benzene 3 h; Heating;
参考文献
Technion Research and Development Foundation Ltd.
Patent: US6908915 B1, 2005 ;
Location in patent: Page/Page column 7-8 ;
参考文献
NOVO NORDISK A/S
Patent: EP820443 B1, 2001 ;
参考文献
Novo Nordisk A/S
Patent: US6239148 B1, 2001 ;
反应条件
sodium borohydride in tetrahydrofuran; n-heptane; water; acetic acid; ethyl acetate
参考文献
Novo Nordisk A/S
Patent: US6239148 B1, 2001 ;
反应条件
boron trifluoride-tetrahydrofuran complex
参考文献
Runyon, Scott P.; Savage, Jason E.; Taroua, Mohamed; Roth, Bryan L.; Glennon, Richard A.; Westkaemper, Richard B.
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 5 p. 655 - 658
反应条件
1: BF3*THF
2: dimethylformamide
3: NaBH4 / propan-2-ol
View Scheme
参考文献
Runyon, Scott P.; Savage, Jason E.; Taroua, Mohamed; Roth, Bryan L.; Glennon, Richard A.; Westkaemper, Richard B.
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 5 p. 655 - 658
