copper(ll) bromide in tetrahydrofuran T=20°C; 0.333333 h;
参考文献
Chemistry Letters, , # 5 p. 466 - 467
→
反应条件
in tetrahydrofuran byproducts: THF; under N2, THF soln. of 1 equiv. of LiOBut in THF was added to 0.064 M soln. of BH3*THF in THF at -78 °C, warming to room temp.; the same result was obtained with mixing at room temp.; monitored by (11)B NMR; LiBH2(OBut)2 and LiB(OBut)4 were not formed;
参考文献
Knizek, Joerg; Noeth, Heinrich; Warchhold, Markus
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2006 , vol. 61, # 9 p. 1079 - 1093
in tetrachloromethane T=20°C; 60 h; in the end the hydronysis by 15percent aqueous THF, other solvent, other time, other temperature; Product distribution;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 54, # 1 p. 100 - 103,87 - 89
