3-乙基-5-己烯-3-醇合成路线 (共 24 条)
反应条件
hydrogenchloride; water in methanol T=20°C;
参考文献
Tetrahedron, , vol. 67, # 11 p. 2081 - 2089
反应条件
zinc in tetrahydrofuran 0.5 h; Ambient temperature;
参考文献
Ranu, Brindaban C.; Majee, Adinath; Das, Asish R.
Tetrahedron Letters, 1995 , vol. 36, # 27 p. 4885 - 4888
反应条件
CH2=CH(Me)Cu(CN)Li2 in tetrahydrofuran T=0°C; 2 h; Yields of byproduct given;
参考文献
Lipshutz, Bruce H.; Wilhelm, Robert S.; Kozlowski, Joseph A.; Parker, David
Journal of Organic Chemistry, 1984 , vol. 49, # 21 p. 3928 - 3938
反应条件
1: biphenyl; propene With lithium in tetrahydrofuran T=25°C; P=760 Torr; 1 h; 2: pentan-3-one in tetrahydrofuran T=-78°C; 0.25 h;
参考文献
Tetrahedron Letters, , vol. 47, # 35 p. 6267 - 6271
反应条件
naphthalene; lithium in tetrahydrofuran T=0°C; 2 h;
参考文献
Guijarro, D.; Mancheno, B.; Yus, M.
Tetrahedron, 1992 , vol. 48, # 22 p. 4593 - 4600
反应条件
AlCl3 etherate in tetrahydrofuran T=-78°C; 1 h;
参考文献
Zhang, Li-Jun; Huang, Yao-Zeng; Jiang, Hong-Xia; Duan-Mu, Jun; Liao, Yi
Journal of Organic Chemistry, 1992 , vol. 57, # 2 p. 774 - 777
反应条件
in diethyl ether T=20°C; 0.5 h;
参考文献
Shen, Kao-Hsien; Yao, Ching-Fa
Journal of Organic Chemistry, 2006 , vol. 71, # 10 p. 3980 - 3983
反应条件
naphthalene; lithium in tetrahydrofuran T=-78 - 0°C; 2 h;
参考文献
Alonso, Emma; Ramon, Diego J.; Yus, Miguel
Tetrahedron, 1996 , vol. 52, # 45 p. 14341 - 14348
反应条件
naphthalene; lithium in tetrahydrofuran T=-78 - 20°C; 5 h;
参考文献
Alonso, Emma; Guijarro, David; Yus, Miguel
Tetrahedron, 1995 , vol. 51, # 9 p. 2699 - 2708
反应条件
naphthalene; lithium in tetrahydrofuran T=0°C; Condensation; 2 h;
参考文献
Alonso, Emma; Guijarro, David; Martinez, Pedro; Ramon, Diego J.; Yus, Miguel
Tetrahedron, 1999 , vol. 55, # 36 p. 11027 - 11038