2,2-二甲基-3-庚酮合成路线 （共 24 条）
反应条件
chloro-trimethyl-silane; CaH2; zinc(II) chloride in tetrahydrofuran T=40°C; 24 h;
参考文献
Tsuhako, Akiko; He, Jing-Qian; Mihara, Mariko; Saino, Naoko; Okamoto, Sentaro
Tetrahedron Letters, 2007 , vol. 48, # 52 p. 9120 - 9123
反应条件
pyridinium chlorochromate in dichloromethane
T=0 - 20°C; 24 h;
参考文献
Hormann, Robert Eugene; Potter, David W.; Chortyk, Orestes; Tice, Colin M.; Carlson, Glenn Richard; Meyer, Andrew; Opie, Thomas R.
Patent: US2006/20146 A1, 2006 ;
Location in patent: Page/Page column 52 ;
反应条件
lithium iodide in various solvent(s)
-78 deg C, 1 h, -78 -> 0 deg C, 1 h;
参考文献
Bertz, Steven H.; Dabbagh, Gary
Tetrahedron, 1989 , vol. 45, # 2 p. 425 - 434
反应条件
in tetrahydrofuran; dichloromethane
T=0°C;
参考文献
Miyasaka, Tadayo; Monobe, Hideaki; Noguchi, Shunsaku
Chemistry Letters, 1986 , p. 449 - 452
反应条件
nitrogen in diethyl ether
-78 deg C to r.t.;
参考文献
Kim, Sunggak; Lee, Jae In; Chung, Bong Young
Journal of the Chemical Society, Chemical Communications, 1981 , # 23 p. 1231 - 1232
反应条件
in chloroform-d1
6 h; Irradiation;
参考文献
Murayama, Hideki; Inoue, Shohei
Chemistry Letters, 1985 , p. 1377 - 1380
反应条件
n-butyllithium; potassium hydride in diethyl ether
参考文献
Bates, Robert B.; Taylor, Stuart R.
Journal of Organic Chemistry, 1994 , vol. 59, # 1 p. 245 - 246
参考文献
Whitmore; Noll; Meunier
Journal of the American Chemical Society, 1939 , vol. 61, p. 684
反应条件
tributylphosphine in tetrahydrofuran
T=20°C; 1 h; Inert atmosphere;
参考文献
Erdik, Ender; Pekel, Oezgen Oemuer
Tetrahedron Letters, 2009 , vol. 50, # 13 p. 1501 - 1503
反应条件
diethyl ether; copper(l) chloride
参考文献
Foley et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 2779,2280
