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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
190835-32-6
合成路线
（共 5 条）
190835-32-6
→
反应条件
207128-61-8
反应条件
diisopropyl-carbodiimide in acetonitrile 16 h; Ambient temperature;
参考文献
Kanaoka, Yoshitomo; Ikeuchi, Yoshihiro; Kawamoto, Tetsuji; Bessho, Kiyoshi; Akimoto, Naoshige; Mikata, Yuji; Nishida, Mamiko; Yano, Shigenobu; Sasaki, Takuma; Yoneda, Fumio
Bioorganic and Medicinal Chemistry, 1998 , vol. 6, # 3 p. 301 - 314
190835-32-6
→
反应条件
207128-62-9
反应条件
1: 62 percent / triethylamine / acetonitrile / 16 h / Ambient temperature 2: 1.3 g / hydrogen / PtO2 / methanol / 1 h / Ambient temperature 3: 26 percent / 1,3-diisopropylcarbodiimide / acetonitrile / 16 h / Ambient temperature View Scheme
参考文献
Kanaoka, Yoshitomo; Ikeuchi, Yoshihiro; Kawamoto, Tetsuji; Bessho, Kiyoshi; Akimoto, Naoshige; Mikata, Yuji; Nishida, Mamiko; Yano, Shigenobu; Sasaki, Takuma; Yoneda, Fumio
Bioorganic and Medicinal Chemistry, 1998 , vol. 6, # 3 p. 301 - 314
190835-32-6
+
207128-68-5
→
反应条件
207128-57-2
反应条件
4-(N,N-dimethlyamino)pyridine in acetonitrile 16 h; Ambient temperature;
参考文献
Kanaoka, Yoshitomo; Ikeuchi, Yoshihiro; Kawamoto, Tetsuji; Bessho, Kiyoshi; Akimoto, Naoshige; Mikata, Yuji; Nishida, Mamiko; Yano, Shigenobu; Sasaki, Takuma; Yoneda, Fumio
Bioorganic and Medicinal Chemistry, 1998 , vol. 6, # 3 p. 301 - 314
190835-32-6
→
反应条件
207128-58-3
反应条件
1: 62 percent / triethylamine / acetonitrile / 16 h / Ambient temperature 2: 1.3 g / hydrogen / PtO2 / methanol / 1 h / Ambient temperature 3: 51 percent / 4-(dimethylamino)pyridine / acetonitrile / 16 h / Ambient temperature View Scheme
参考文献
Kanaoka, Yoshitomo; Ikeuchi, Yoshihiro; Kawamoto, Tetsuji; Bessho, Kiyoshi; Akimoto, Naoshige; Mikata, Yuji; Nishida, Mamiko; Yano, Shigenobu; Sasaki, Takuma; Yoneda, Fumio
Bioorganic and Medicinal Chemistry, 1998 , vol. 6, # 3 p. 301 - 314
207128-72-1
→
反应条件
190835-32-6
反应条件
<b>Multi-step reaction with 3 steps<br /> </b>1: 952 mg / hydrogen / PtO<sub>2</sub> / methanol / 1 h / Ambient temperature; other catalyst: Pd-C<br />2: 78 percent / triethylamine / tetrahydrofuran / 16 h / Ambient temperature<br />3: 910 mg / hydrogen / PtO<sub>2</sub> / methanol / 1 h / Ambient temperature<br /> <br />
参考文献
Kanaoka, Yoshitomo; Ikeuchi, Yoshihiro; Kawamoto, Tetsuji; Bessho, Kiyoshi; Akimoto, Naoshige; Mikata, Yuji; Nishida, Mamiko; Yano, Shigenobu; Sasaki, Takuma; Yoneda, Fumio Bioorganic and Medicinal Chemistry, 1998 , vol. 6, # 3 p. 301 - 314
