(S)-4-苯基噁唑烷-2-硫酮合成路线 (共 5 条)
反应条件
dihydrogen peroxide; potassium carbonate in ethanol T=50°C;
参考文献
Wu, Yikang; Yang, Yong-Qing; Hu, Qi
Journal of Organic Chemistry, 2004 , vol. 69, # 11 p. 3990 - 3992
反应条件
Birman's catalyst; methanol; benzoic acid in chloroform-d1 T=20°C; 48 h; Resolution of racemate; enantioselective reaction;
参考文献
Organic Letters, , vol. 15, # 11 p. 2790 - 2793
反应条件
1: (S)-1-phenyl-2-hydroxyethylamine With sulfuric acid T=0°C; 2 h; 2: potassium ethylxanthate With sodium hydroxide; sulfuric acid T=50°C; pH=9; 9 h;
参考文献
Tetrahedron, , vol. 57, # 43 p. 8939 - 8949
反应条件
1: (rac)-4-phenyl-1,3-oxazolidine-2-thione With Birman's catalyst; N-ethyl-N,N-diisopropylamine in chloroform T=23°C; Resolution of racemate; 2: isobutyric anhydride With sodium sulfate in chloroform T=23°C; 1 h; Resolution of racemate; enantioselective reaction;
参考文献
Journal of the American Chemical Society, , vol. 134, # 42 p. 17605 - 17612
反应条件
lithium hydroxide monohydrate; water in tetrahydrofuran optical yield given as percent eeenantioselective reaction;
参考文献
Synlett, , # 6 p. 960 - 964