(R,R)-N-lt;3,5-di-t-butyl-6-(11-(silica-O-SiMe2-linked)undecyloxy)gt;benzylidene-N'-(3-t-butyl-2,5-dihydroxy)benzylidene-1,2-cyclohexanediamine - (acetoxy)Co; water in tetrahydrofuran Ambient temperature; Yield givenYields of byproduct given. Title compound not separated from byproducts;

1,3-benzenedicarboxylic acid; tri-n-butyltin methoxide 1.) 120 deg C, 25 Hgmm 2.)180-200 deg C; Yield given. Multistep reaction;

1,3-benzenedicarboxylic acid; tri-n-butyltin methoxide 1.) 120 deg C, 25 Hgmm 2.)180-200 deg C; Yield given. Multistep reaction;

(R,R)-N-lt;3,5-di-t-butyl-6-(11-(silica-O-SiMe2-linked)undecyloxy)gt;benzylidene-N'-(3-t-butyl-2,5-dihydroxy)benzylidene-1,2-cyclohexanediamine - (acetoxy)Co; water in tetrahydrofuran Ambient temperature; Yield givenYields of byproduct given. Title compound not separated from byproducts;

indium(III) chloride; 1-n-butyl-3-methylimidazolium hexafluorophosphate T=20°C; 4 h;

暂无反应条件数据

byproducts: C2H5OH; heating equimolar amts. of educts; remove alc.;

byproducts: CH3OH; heating equimolar amts. of educts; remove alc.;