4,4’-双叔丁基二苯基甲烷合成路线 （共 28 条）
反应条件
1: 54 percent / periodic acid, 98percent H2SO4 / H2O 2: 95 percent / copper / 4 h / 230 °C 3: 92 percent / N-bromosuccinimide / various solvent(s) / 6 h / 70 - 75 °C View Scheme
参考文献
Kajigaeshi, Shoji; Kadowaki, Toshiya; Nishida, Akiko; Fujisaki, Shizuo
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 97 - 104
反应条件
copper(II) nitrate in acetic anhydride T=60°C; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 46, # 11 p. 2376 - 2379
反应条件
copper(II) nitrate T=60°C; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 46, # 11 p. 2376 - 2379
反应条件
nitric acid T=-50°C; 1 h; other temperatures; further nitration agents; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 46, # 11 p. 2376 - 2379
反应条件
water; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; iron(II) chloride T=60°C; 5 h;
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 28 p. 6971 - 6975
反应条件
(i) 1,1-diphenyl-ethyl hydroperoxide, Na2CO3, (ii) H2SO4; Multistep reaction;
参考文献
Pisanenko,D.A.; Zavgorodnii,S.V.
Sov. Prog. Chem. (Engl. Transl.), 1968 , vol. 34, # 3 p. 280 - 284,38 - 40
反应条件
in tetrahydrofuran T=30°C; Equilibrium constant;
参考文献
Ahlbrecht, Hubertus; Schneider, Gunther
Tetrahedron, 1986 , vol. 42, # 17 p. 4729 - 4742
反应条件
1: I2, HIO4, H2SO4, H2O / acetic acid / 24 h / 70 - 78 °C 2: 85 percent / Zn / NiCl2(PPh3)2, PPh3 / dimethylformamide / 24 h / 70 - 75 °C View Scheme
参考文献
Kajigaeshi, Shoji; Kadowaki, Toshiya; Nishida, Akiko; Fujisaki, Shizuo
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 97 - 104
反应条件
1: 54 percent / periodic acid, 98percent H2SO4 / H2O 2: 95 percent / copper / 4 h / 230 °C 3: 84 percent / iron, chlorine / CCl4 / 0.5 h / 30 °C 4: 37 percent / AlCl3 / benzene / 0.5 h / 50 °C View Scheme
参考文献
Kajigaeshi, Shoji; Kadowaki, Toshiya; Nishida, Akiko; Fujisaki, Shizuo
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 97 - 104
反应条件
in tetrahydrofuran T=30°C; Equilibrium constant;
参考文献
Tetrahedron, , vol. 42, # 17 p. 4729 - 4742
