2-(1,3-二甲基咪唑烷-2-亚基)-1,3-二甲基-咪唑烷合成路线 （共 12 条）
反应条件
T=60°C; P=0.1 Torr; Yield given;
参考文献
Denk; Thadani; Hatano; Lough
Angewandte Chemie - International Edition in English, 1997 , vol. 36, # 23 p. 2607 - 2609
反应条件
1: K / tetrahydrofuran / 0.5 h / Heating 2: 60 °C / 0.1 Torr View Scheme
参考文献
Denk; Thadani; Hatano; Lough
Angewandte Chemie - International Edition in English, 1997 , vol. 36, # 23 p. 2607 - 2609
反应条件
Mes3SiCl in toluene T=-60°C; 16 h; Irradiation;
参考文献
Neumann, Wilhelm P.; Schultz, Klaus-Dieter; Vieler, Robert
Journal of Organometallic Chemistry, 1984 , vol. 264, # 1-2 p. 179 - 192
反应条件
in toluene Irradiation (UV/VIS); a soln. of chlorogermane and diimidazolidine irradiating for 20 h at -55°C, cold MeOH adding, digermane ppt. sepg., washing with cold MeOH under Ar, drying in vacuo at room temp.; identified by elem. anal., IR, UV, NMR and mass spectra;
参考文献
Neumann, Wilhelm P.; Schultz, Klaus-Dieter; Vieler, Robert
Journal of Organometallic Chemistry, 1984 , vol. 264, # 1-2 p. 179 - 192
反应条件
in toluene Irradiation (UV/VIS); a soln. of chlorogermane and diimidazolidine irradiating for 20 h at -60°C, cold MeOH adding, digermane ppt. sepg., washing with cold MeOH under Ar, drying in vacuo at room temp.; identified by elem. anal., IR, NMR and mass spectra;
参考文献
Neumann, Wilhelm P.; Schultz, Klaus-Dieter; Vieler, Robert
Journal of Organometallic Chemistry, 1984 , vol. 264, # 1-2 p. 179 - 192
反应条件
in toluene Irradiation (UV/VIS); a soln. of chlorogermane and diimidazolidine irradiating for 20 h at -60°C, cold MeOH adding, digermane ppt. sepg., washing with cold MeOH under Ar, drying in vacuo at room temp.; identified by elem. anal., IR, UV, NMR and mass spectra;
参考文献
Neumann, Wilhelm P.; Schultz, Klaus-Dieter; Vieler, Robert
Journal of Organometallic Chemistry, 1984 , vol. 264, # 1-2 p. 179 - 192
反应条件
in toluene Irradiation (UV/VIS); a soln. of chlorogermane and diimidazolidine irradiating for 20 h at -60°C, cold MeOH adding, digermane ppt. sepg., washing with cold MeOH under Ar, drying in vacuo at room temp.; identified by elem. anal., IR, UV, NMR and mass spectra;
参考文献
Neumann, Wilhelm P.; Schultz, Klaus-Dieter; Vieler, Robert
Journal of Organometallic Chemistry, 1984 , vol. 264, # 1-2 p. 179 - 192
反应条件
in toluene Irradiation (UV/VIS); a soln. of chlorogermane and diimidazolidine irradiating for 20 h at -70°C, cold MeOH adding, digermane ppt. sepg., washing with cold MeOH under Ar, drying in vacuo at room temp.; identified by elem. anal., IR, UV, NMR and mass spectra;
参考文献
Neumann, Wilhelm P.; Schultz, Klaus-Dieter; Vieler, Robert
Journal of Organometallic Chemistry, 1984 , vol. 264, # 1-2 p. 179 - 192
反应条件
in toluene Irradiation (UV/VIS); a soln. of chlorogermane and diimidazolidine irradiating for 20 h at room temp., MeOH adding, digermane ppt. sepg., washing with cold MeOH under Ar, drying in vacuo at room temp.; identified by elem. anal., IR, NMR and mass spectra;
参考文献
Neumann, Wilhelm P.; Schultz, Klaus-Dieter; Vieler, Robert
Journal of Organometallic Chemistry, 1984 , vol. 264, # 1-2 p. 179 - 192
参考文献
Cetinkaya, Bekir; Cetinkaya, Engin; Kuecuekbay, Hasan; Durmaz, Riza
Arzneimittel-Forschung/Drug Research, 1996 , vol. 46, # 12 p. 1154 - 1158
