(2-氯苯甲酰)乙酸乙酯合成路线 (共 15 条)
反应条件
1: 81 percent / Ac2O / montmorillonite K-10 / 8 h / 130 - 140 °C 2: 85 percent / acetonitrile / 3 h / Heating 3: NaH / dioxane / 3.5 h / Heating 4: 0.324 g / KOH / methanol; H2O / 3 h / Heating View Scheme
参考文献
Grohe, Klaus; Heitzer, Helmut
Liebigs Annalen der Chemie, 1987 , p. 29 - 37
反应条件
1: 81 percent / Ac2O / montmorillonite K-10 / 8 h / 130 - 140 °C 2: 74 percent / acetonitrile / 3 h / Heating 3: NaH / dioxane / 3.5 h / Heating 4: KOH / methanol; H2O / 3 h / Heating View Scheme
参考文献
Sayyed; Panse; Bhawal; Deshmukh
Synthetic Communications, 2000 , vol. 30, # 14 p. 2533 - 2540
参考文献
Thorp; Brunskill
Journal of the American Chemical Society, 1915 , vol. 37, p. 1262
参考文献
Thorp; Brunskill
Journal of the American Chemical Society, 1915 , vol. 37, p. 1262
反应条件
1: SO2Cl2
2: 31 percent / ethanol / 16 h / Heating
View Scheme
参考文献
Lee, Len F.; Schleppnik, Francis M.; Howe, Robert K.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 1621 - 1630