1-(2-氯苯基)-2-丙炔-1-醇合成路线 （共 5 条）
反应条件
Yield given. Multistep reaction;
参考文献
Wang, Yan; Zheng, Kuan; Hong, Ran
Journal of the American Chemical Society, 2012 , vol. 134, # 9 p. 4096 - 4099
反应条件
1.1: n-butyllithium / tetrahydrofuran / 1.5 h / -70 °C / Inert atmosphere 1.2: 1.5 h / -70 - 20 °C / Inert atmosphere 1.3: 0 °C 2.1: methanol; potassium carbonate / 12 h / 20 °C / Inert atmosphere View Scheme
参考文献
Ghosh, Nayan; Nayak, Sanatan; Sahoo, Akhila K.
Journal of Organic Chemistry, 2011 , vol. 76, # 2 p. 500 - 511
反应条件
sodium hydroxide; n-butyllithium 1.) THF, -78 deg C, 1 h; 2.) methanol, 30 min; 3.) CH2Cl2, 2-3 h, sunlight; Yield given. Multistep reaction;
参考文献
Baldoli, Clara; Del Buttero, Paola; Licandro, Emanuela; Maiorana, Stefano; Papagni, Antonio; Torchio, Maurizio
Tetrahedron Letters, 1993 , vol. 34, # 49 p. 7943 - 7946
反应条件
2.) atmosphere 1.) THF, -15 deg C, 1 h; 2.) CH2Cl2, 2-3 h, sunlight; Yield given. Multistep reaction;
参考文献
Baldoli, Clara; Del Buttero, Paola; Licandro, Emanuela; Maiorana, Stefano; Papagni, Antonio; Torchio, Maurizio
Tetrahedron Letters, 1993 , vol. 34, # 49 p. 7943 - 7946
反应条件
diethyl ether; ammonia
参考文献
Johnson
Journal of the Chemical Society, 1947 , p. 1626,1630
