1'-羟基-2',3'-去氢草蒿脑合成路线 （共 29 条）
反应条件
1: Jones reagent
2: 9 percent / 8 h / Ambient temperature; Irradiation
View Scheme
参考文献
Nishio, Takehiko; Nakata, Hiroyuki; Omote, Yoshimori
Journal of Heterocyclic Chemistry, 1986 , vol. 23, p. 1011 - 1013
反应条件
1: Jones reagent
2: 12 percent / 8 h / Ambient temperature; Irradiation
View Scheme
参考文献
Nishio, Takehiko; Nakata, Hiroyuki; Omote, Yoshimori
Journal of Heterocyclic Chemistry, 1986 , vol. 23, p. 1011 - 1013
反应条件
lithium aluminium tetrahydride; aluminium trichloride
参考文献
Fleming, Steven A.; Carroll, Sean M.; Hirschi, Jennifer; Liu, Renmao; Pace, J. Lee; Redd, J. Ty
Tetrahedron Letters, 2004 , vol. 45, # 17 p. 3341 - 3343
反应条件
1: 94 percent / CrO3, H2SO4
2: 51 percent / CuI, PPh3, K2CO3 / dimethylformamide / 10 h / 100 - 120 °C
View Scheme
参考文献
Kundu, Nitya G.; Pal, Manojit; Chowdhury, Chinmay
Journal of Chemical Research, Miniprint, 1995 , # 1 p. 101 - 123
反应条件
1: 79 percent / H2 / Pb/5percent Pd/CaCO3 / 36 h / Ambient temperature
2: 79 percent / Jones' reagent / acetone / 0.5 h / 0 °C
View Scheme
参考文献
Kundu; Dasgupta; Chaudhuri; Mahanty; Spears; Shahinian
European Journal of Medicinal Chemistry, 1993 , vol. 28, # 6 p. 473 - 479
反应条件
1: 1-(p-methoxy)phenyl propargyl alcohol With palladium diacetate; gold(I) chloride in nitromethane
T=20°C; 0.0833333 h; Inert atmosphere;
2: thiophenol in nitromethane
T=80°C; 24 h; Inert atmosphere; regioselective reaction;
参考文献
Biswas, Srijit; Watile, Rahul A.; Samec, Joseph S. M.
Chemistry - A European Journal, 2014 , vol. 20, # 8 p. 2159 - 2163
反应条件
1: 83 percent / Pd(PPh3)2Cl2; CuI; Et3N / dimethylformamide / 24 h / 20 °C
2: 70 percent / p-toluenesulfonic acid / benzene / 24 h / 20 °C
3: 61 percent / p-toluenesulfonic acid / benzene / 8 h / Heating
View Scheme
参考文献
De, Mahuya; Majumdar, Dyuti P.; Kundu, Nitya G.
Journal of the Indian Chemical Society, 1999 , vol. 76, # 11-12 p. 665 - 674
反应条件
1: Jones reagent
2: 7 percent / 8 h / Ambient temperature; Irradiation
View Scheme
参考文献
Nishio, Takehiko; Nakata, Hiroyuki; Omote, Yoshimori
Journal of Heterocyclic Chemistry, 1986 , vol. 23, p. 1011 - 1013
反应条件
hydrogen; Lindlar's catalyst; α-[2-(2-butoxyethoxy)ethoxy]-4,5-methylenedioxy-2-propyltoluene
36 h; Ambient temperature;
参考文献
Kundu; Dasgupta; Chaudhuri; Mahanty; Spears; Shahinian
European Journal of Medicinal Chemistry, 1993 , vol. 28, # 6 p. 473 - 479
