雄甾-3,5-二烯-17-酮合成路线 (共 5 条)
反应条件
1: ethanol; palladium / Hydrogenation 3: sodium ethylate solution / 200 °C View Scheme
参考文献
Burrows et al.
Biochemical Journal, 1937 , vol. 31, p. 950,957
反应条件
pyridin-2-yl hydrobromide T=25 - 30°C; 6 h;
参考文献
CHORISIS S.R.L.
Patent: WO2009/59765 A2, 2009 ;
Location in patent: Page/Page column 5-6 ;
反应条件
1: 14 percent / 85percent m-chloroperbenzoic acid / benzene / 120 h / 20 °C 2: 74 percent / 10percent KOH / methanol / 1 h / Heating View Scheme
参考文献
Cambie, Richard C.; Read, Christine M.; Rutledge, Peter S.; Walker, Geoffrey J.; Woodgate, Paul D.; Hanson, James R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2581 - 2586
反应条件
chromic acid in acetone T=0 - 20°C; Oxidation;
参考文献
Journal of Chemical Research, Miniprint, , # 10 p. 2532 - 2545
参考文献
Rosenkranz; Kaufmann; Romo
Journal of the American Chemical Society, 1949 , vol. 71, p. 3689,3692
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Wolfe; Fieser; Friedgood
Journal of the American Chemical Society, 1941 , vol. 63, p. 582,592
Full Text Show Details
Burrows et al.
Biochemical Journal, 1937 , vol. 31, p. 950,957