反应条件
1: NCS, aq. AgNO3, 2,4,6-collidine / acetonitrile / 0.02 h / 0 °C 2: 65 percent / NaBH(OAc)3 / acetonitrile; acetic acid / 5 h / 0 °C 3: 82 percent / TBAF / tetrahydrofuran / Ambient temperature 4: 87 percent / MnO2 / CH2Cl2 / 3 h / Ambient temperature View Scheme
参考文献
Chida, Noritaka; Yoshinaga, Mitsukane; Tobe, Takahiko; Ogawa, Seiichiro
Chemical Communications, 1997 , # 11 p. 1043 - 1044
