[PdCl2((S)-(CH3OC6H3P(C6H5)2)2)]; silver carbonate in N,N-dimethyl-formamide T=50°C; 168 h;
参考文献
Trabesinger, Gerald; Albinati, Alberto; Feiken, Nantko; Kunz, Roland W.; Pregosin, Paul S.; Tschoerner, Matthias
Journal of the American Chemical Society, 1997 , vol. 119, # 27 p. 6315 - 6323
tris(dibenzylideneacetone)dipalladium (0); (S)-(6,6'-dimethoxy[1,1'-biphenyl]-2,2'-diyl)bis[bis(3,5-di-tert-butyl-phenyl)-phosphine]; N-ethyl-N,N-diisopropylamine in tetrahydrofuran T=70°C; 168 h;
参考文献
Trabesinger, Gerald; Albinati, Alberto; Feiken, Nantko; Kunz, Roland W.; Pregosin, Paul S.; Tschoerner, Matthias
Journal of the American Chemical Society, 1997 , vol. 119, # 27 p. 6315 - 6323
N,N,N',N'-tetra-methylnaphthalene-1,8-diamine; tris-(dibenzylideneacetone)dipalladium(0); (R)-(+)-2,2'-bis(diphenylphosphino)-3,3'-bi(benzo[b]thiophen) in N,N-dimethyl-formamide T=90°C; Arylation; Heck reaction; 18 h; Title compound not separated from byproducts;
参考文献
Gibson, Susan E.; Ibrahim, Hasim; Pasquier, Corinne; Swamy, Vishwanath M.
Tetrahedron Asymmetry, 2003 , vol. 14, # 11 p. 1455 - 1458
chiral phosphorus reagent; N-ethyl-N,N-diisopropylamine; tris(dibenzylideneacetone)dipalladium (0) in ethylene glycol dimethyl ether T=85°C; Heck arylation reaction; Further byproducts given. Title compound not separated from byproducts;
参考文献
Andersen, Nell G.; Parvez, Masood; McDonald, Robert; Keay, Brian A.
Canadian Journal of Chemistry, 2004 , vol. 82, # 2 p. 145 - 161
