(E)-4-(4-甲氧基苯基)丁-2-酮肟合成路线 （共 6 条）
反应条件
1: 76 percent / trifluoromethanesulfonic acid; Molecular Sieves 5A / tetrabutylammonium perrhenate / 1,2-dichloro-ethane / 1 h / Heating 2: 75 percent / chloranil; CF3SO3H / nitrobenzene / 6 h / 120 °C View Scheme
参考文献
Kusama; Yamashita; Uchiyama; Narasaka
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 5 p. 965 - 975
反应条件
chloranil; trifluoroacetic anhydride in dichloromethane T=20°C; 21 h;
参考文献
Kitamura, Mitsuru; Yoshida, Masayuki; Kikuchi, Takashi; Narasaka, Koichi
Synthesis, 2003 , # 15 p. 2415 - 2426
反应条件
1: 94 percent Spectr. / (CF3CO)2O / CH2Cl2 / 20 °C 2: 73.4 mg / 4-chloranil / CH2Cl2 / 21 h / 20 °C View Scheme
参考文献
Kitamura, Mitsuru; Yoshida, Masayuki; Kikuchi, Takashi; Narasaka, Koichi
Synthesis, 2003 , # 15 p. 2415 - 2426
反应条件
chloranil; trifluoroacetic anhydride in dichloromethane T=20°C; 21 h;
参考文献
Kitamura, Mitsuru; Yoshida, Masayuki; Kikuchi, Takashi; Narasaka, Koichi
Synthesis, 2003 , # 15 p. 2415 - 2426
反应条件
1: 94 percent Spectr. / (CF3CO)2O / CH2Cl2 / 20 °C
2: 4-chloranil / CH2Cl2 / 21 h / 20 °C
View Scheme
参考文献
Kitamura, Mitsuru; Yoshida, Masayuki; Kikuchi, Takashi; Narasaka, Koichi
Synthesis, 2003 , # 15 p. 2415 - 2426
反应条件
trifluoroacetic anhydride in dichloromethane
T=20°C;
参考文献
Kitamura, Mitsuru; Yoshida, Masayuki; Kikuchi, Takashi; Narasaka, Koichi
Synthesis, 2003 , # 15 p. 2415 - 2426
