1,2-二氢-3,3-二甲基-2-氧代-3H-吲哚合成路线 （共 72 条）
反应条件
copper(I) oxide; 1,2-diamino-benzene; sodium t-butanolate in tert-butyl alcohol T=100°C; 18 h; Sealed tube;
参考文献
Jhan, Yu-Huei; Kang, Ting-Wei; Hsieh, Jen-Chieh
Tetrahedron Letters, 2013 , vol. 54, # 9 p. 1155 - 1159
反应条件
hydrogenchloride in water 1 h; Reflux;
参考文献
BOEHRINGER INGELHEIM INTERNATIONAL GMBH
Patent: US2011/195954 A1, 2011 ;
Location in patent: Page/Page column 86 ;
反应条件
palladium diacetate; hydrogen; tri-cyclo-hexyl-phosphine in dichloromethane T=100°C; P=31028.9 Torr; 48 h;
参考文献
El Ali, Bassam; Okuro, Kazumi; Vasapollo, Giuseppe; Alper, Howard
Journal of the American Chemical Society, 1996 , vol. 118, # 18 p. 4264 - 4270
反应条件
n-butyllithium; lithium chloride in tetrahydrofuran
参考文献
McComas, Casey C.; Vu, An T.; Mahaney, Paige E.; Cohn, Stephen T.; Fensome, Andrew; Marella, Michael A.; Nogle, Lisa; Trybulski, Eugene J.; Ye, Fei; Zhang, Puwen; Alfinito, Peter; Bray, Jenifer; Johnston, Grace; Koury, Elizabeth; Deecher, Darlene C.
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 18 p. 4929 - 4931
反应条件
samarium diiodide in tetrahydrofuran; water T=0°C; 1 h;
参考文献
Wasa, Masayuki; Yu, Jin-Quan
Journal of the American Chemical Society, 2008 , vol. 130, # 43 p. 14058 - 14059
反应条件
AlCl3, aluminium chloride T=90 - 120°C; 0.5 h;
参考文献
Uchida, Chikara; Sone, Hiroki; Kawamura, Kiyoshi
Patent: US2006/194842 A1, 2006 ;
Location in patent: Page/Page column 40 ;
US 20060194842 A1
反应条件
copper(l) iodide; N-acetyl-glycine; potassium iodide; sodium hydroxide in tert-butyl alcohol T=100°C; 24 h;
参考文献
Hsieh, Jen-Chieh; Cheng, An-Yi; Fu, Jun-Hao; Kang, Ting-Wei
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 31 p. 6404 - 6409
反应条件
copper(l) iodide; 1,2-diamino-benzene; sodium t-butanolate in tert-butyl alcohol T=100°C; 24 h; Sealed tube; Reagent/catalystSolventTemperature;
参考文献
Jhan, Yu-Huei; Kang, Ting-Wei; Hsieh, Jen-Chieh
Tetrahedron Letters, 2013 , vol. 54, # 9 p. 1155 - 1159
反应条件
18-crown-6 ether; potassium tert-butylate in tetrahydrofuran T=-78 - 20°C; 4 h;
参考文献
US2005/261244 A1, ;
Page/Page column 52 ;
US 20050261244 A1
反应条件
copper(I) oxide; 1,2-diamino-benzene; sodium t-butanolate in tert-butyl alcohol T=100°C; 4 h; Sealed tube; Time;
参考文献
Tetrahedron Letters, , vol. 54, # 9 p. 1155 - 1159
