2-苯基-2H-苯并噻唑合成路线 （共 42 条）
反应条件
in various solvent(s)
0.5 h; Heating;
参考文献
Houghton, Peter G.; Pipe, David F.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1471 - 1480
反应条件
sodium hydroxide; Cu(II) phenylcyclopropyl carboxylate; palladium diacetate; (tppts)2 in water
T=100°C; 6 h; withou Cu salt, without Pd catalyst; Product distribution;
参考文献
Beletskaya, Irina P.; Davydov, Dmitri V.; Moreno-Manas, Marcial
Tetrahedron Letters, 1998 , vol. 39, # 31 p. 5621 - 5622
反应条件
1: benzene / 0.08 h / Ambient temperature
2: mercuric oxide, magnesium dioxide
3: various solvent(s) / Heating
View Scheme
参考文献
Houghton, Peter G.; Pipe, David F.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1471 - 1480
反应条件
1: acetic acid / 40 h / 85 °C
2: sodium azide; copper(l) iodide; N,N,N',N,-tetramethylethylenediamine; N-hexadecyl-N,N,N-trimethylammonium bromide / water / 16 h / 130 °C / |Sealed tube; |Inert atmosphere
View Scheme
参考文献
Shang, Xiaobo; Zhao, Shixian; Chen, Wanzhi; Chen, Chao; Qiu, Huayu
Chemistry - A European Journal, 2014 , vol. 20, # 7 p. 1825 - 1828
反应条件
1: acetic acid / 40 h / 85 °C
2: sodium azide; copper(l) iodide; N,N,N',N,-tetramethylethylenediamine; N-hexadecyl-N,N,N-trimethylammonium bromide / water / 16 h / 130 °C / |Sealed tube; |Inert atmosphere
View Scheme
参考文献
Shang, Xiaobo; Zhao, Shixian; Chen, Wanzhi; Chen, Chao; Qiu, Huayu
Chemistry - A European Journal, 2014 , vol. 20, # 7 p. 1825 - 1828
参考文献
Shi, Suping; Liu, Wei; He, Ping; Kuang, Chunxiang
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 22 p. 3576 - 3580
反应条件
in various solvent(s)
Heating; Yield given;
参考文献
Houghton, Peter G.; Pipe, David F.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1471 - 1480
反应条件
sulfuric acid
Diazotization.Erwaermen der Diazoniumsulfat-Loesung mit Alkohol;
参考文献
Kehrmann; Messinger
Chemische Berichte, 1892 , vol. 25, p. 899
反应条件
in diphenylether
6 h; Heating;
参考文献
Houghton, Peter G.; Pipe, David F.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1471 - 1480
反应条件
1: hydrochloride of aniline / 40 °C
View Scheme
参考文献
Gattermann; Wichmann
Chemische Berichte, 1888 , vol. 21, p. 1636
