反应条件
1: 50 percent / Jones reagent / acetone / 3 h / 0 - 20 °C
2: 1.) N-methylmorpholine, isobutyl chloroformate, 2.) N-hydroxy-2-thiopyridone, Et3N / 1.) THF, -15 deg C, 15 min, 2.) Et2O, THF, -15 deg C, 1 h
View Scheme
参考文献
Diaz, Adolfo; Siro, Jorge G.; Garcia-Navio, Jose L.; Vaquero, Juan J.; Alvarez-Builla, Julio
Synthesis, 1997 , # 5 p. 559 - 562
