2-[(三氟乙酰基)氨基]苯甲酸钠合成路线 （共 9 条）
反应条件
T=20°C; 2.25 h; Cooling with ice;
参考文献
Neves Filho, Ricardo A. W.; Stark, Sebastian; Westermann, Bernhard; Wessjohann, Ludger A.
Beilstein Journal of Organic Chemistry, 2012 , vol. 8, p. 2085 - 2090
反应条件
in tetrahydrofuran T=20°C; 2 h;
参考文献
Emenike, Bright U.; Liu, Albert Tianxiang; Naveo, Elsy P.; Roberts, John D.
Journal of Organic Chemistry, 2013 , vol. 78, # 23 p. 11765 - 11771
反应条件
1: DMAP; DCC / acetonitrile / 24 h / 40 °C 2: 426 mg / NaBH4 / ethanol / 2 h View Scheme
参考文献
Barker, David; McLeod, Malcolm D.; Brimble, Margaret A.; Savage, G. Paul
Tetrahedron Letters, 2001 , vol. 42, # 9 p. 1785 - 1788
反应条件
1: DMAP; DCC / acetonitrile / 24 h / 40 °C 2: 893 mg / NaBH4 / ethanol / 2 h View Scheme
参考文献
Barker, David; McLeod, Malcolm D.; Brimble, Margaret A.; Savage, G. Paul
Tetrahedron Letters, 2001 , vol. 42, # 9 p. 1785 - 1788
反应条件
1: Ac2O / 1 h / Heating 2: AcONH4 / 7 h / 220 °C 3: POCl3 / 3 h / Heating View Scheme
参考文献
Palanki, Moorthy S. S.; Erdman, Paul E.; Ren, Minghuan; Suto, Mark; Bennett, Brydon L.; Manning, Anthony; Ransone, Lynn; Spooner, Cheryl; Desai, Sonal; Ow, Arnie; Totsuka, Ryuichi; Tsao, Peter; Toriumi, Wataru
Bioorganic and Medicinal Chemistry Letters, 2003 , vol. 13, # 22 p. 4077 - 4080
反应条件
1,1'-carbonyldiimidazole 1.) 2 h, RT; 2.) tert-butyl alcohol, 36 h, RT, and ethanol, sodium borohydride, 0 deg C, ca. 25 min; Yield given. Multistep reaction;
参考文献
Schepartz, Alanna; Breslow, Ronald
Journal of the American Chemical Society, 1987 , vol. 109, # 6 p. 1814 - 1826
反应条件
1: DMAP; DCC / acetonitrile / 24 h / 40 °C 2: NaBH4 / ethanol / 2 h View Scheme
参考文献
Barker, David; McLeod, Malcolm D.; Brimble, Margaret A.; Savage, G. Paul
Tetrahedron Letters, 2001 , vol. 42, # 9 p. 1785 - 1788
反应条件
thionyl chloride in benzene 21.5 h; Heating;
参考文献
Palanki, Moorthy S. S.; Erdman, Paul E.; Ren, Minghuan; Suto, Mark; Bennett, Brydon L.; Manning, Anthony; Ransone, Lynn; Spooner, Cheryl; Desai, Sonal; Ow, Arnie; Totsuka, Ryuichi; Tsao, Peter; Toriumi, Wataru
Bioorganic and Medicinal Chemistry Letters, 2003 , vol. 13, # 22 p. 4077 - 4080
反应条件
sulfuric acid; nitric acid
T=10°C;
参考文献
Broxton, Trevor J.
Australian Journal of Chemistry, 1983 , vol. 36, # 9 p. 1885 - 1893
