in neat (no solvent) byproducts: dimethylamine; 120°C, 5h;
参考文献
Brown,M.P. et al.
Journal of the Chemical Society, 1962 , p. 4648 - 4652
Full Text View citing articles Show Details
Gmelin Handbook: B: B-Verb.1, 2.5.2.2, page 130 - 132
N(C2H5)3 in hexane byproducts: ((C2H5)3NH)Cl; under N2, addn. of both amines in hexane to a stirred hexane soln. of B-compd. at -30°C, refluxed for 17 h; centrifugation, hexane evapd., fractional distn.;
in hexane under N2, addn. of B-compd. in hexane to Li-compd. in hexane at -60°C with stirring, allowed to attain ambient temp.; insoluble material removed, hexane removed, fractional distn.;
