3-氯-2,4-二甲基戊烷合成路线 (共 3 条)
反应条件
trichloroacetonitrile; triphenylphosphine in acetonitrile T=-15 - 20°C;
参考文献
Graf, Claus-Dieter; Malan, Christophe; Harms, Klaus; Knochel, Paul
Journal of Organic Chemistry, 1999 , vol. 64, # 15 p. 5581 - 5588
反应条件
tetrachloromethane; 4-(N,N-dimethlyamino)pyridine; Fonderma 3 h; Heating;
参考文献
Stofer, Edmond; Lion, Claude
Bulletin des Societes Chimiques Belges, 1987 , vol. 96, # 8 p. 623 - 628
反应条件
trichloroacetonitrile; triphenylphosphine in 1,2-dichloro-benzene T=-7°C; 24 h; other alcohols; other halogenating agents; also with use of iodide and thiocyanate ions; var. solvents, temp. and reaction times; Product distribution;
参考文献
Matveeva, E. D.; Yalovskaya, A. I.; Cherepanov, I. A.; Bundel', Yu. G.; Kurts, A. L.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 8.1 p. 1409 - 1415
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 8 p. 1611 - 1618