2-甲基-5,6,7,8-四氢-3H-喹唑啉-4-酮合成路线 (共 7 条)
反应条件
caesium carbonate in N,N-dimethyl-formamide T=20°C; 10 h; Inert atmosphereSealed tube;
参考文献
Yu, Lin; Wang, Min; Li, Pinhua; Wang, Lei
Applied Organometallic Chemistry, 2012 , vol. 26, # 11 p. 576 - 582,7
反应条件
potassium carbonate in methanol
参考文献
Meiji Seika Kaisha, Ltd.
Patent: EP1142881 A1, 2001 ;
反应条件
palladium on activated charcoal in toluene 0.5 h; Heating;
参考文献
Fueloep, Ferenc; Bernath, Gabor
Synthesis, 1985 , # 12 p. 1148 - 1149
参考文献
American Home Products Corporation
Patent: US5234936 A1, 1993 ;
参考文献
Baumgarten et al.
Journal of the American Chemical Society, 1958 , vol. 80, p. 6609,6611
反应条件
1: NOBF4 / |Inert atmosphere 2: phosphorus trichoride / chloroform / 2 h / |Inert atmosphere; |Reflux 3: aluminum oxide / |Inert atmosphere View Scheme
参考文献
Sedenkova, Kseniya N.; Averina, Elena B.; Grishin, Yuri K.; Kuznetsova, Tamara S.; Zefirov, Nikolay S.
Tetrahedron Letters, 2014 , vol. 55, # 2 p. 483 - 485
反应条件
1: phosphorus trichoride / chloroform / 2 h / |Inert atmosphere; |Reflux 2: aluminum oxide / |Inert atmosphere View Scheme
参考文献
Sedenkova, Kseniya N.; Averina, Elena B.; Grishin, Yuri K.; Kuznetsova, Tamara S.; Zefirov, Nikolay S.
Tetrahedron Letters, 2014 , vol. 55, # 2 p. 483 - 485