双(十二烷基环戊二烯)二氯化锆合成路线 (共 1 条)
反应条件
1: CpMgCl; dodecyl bromide in tetrahydrofuran T=60°C; 6 h; Inert atmosphere; 2: With n-butyllithium in hexanes; diethyl ether T=20°C; 0.666667 h; Inert atmosphere; 3: zirconium tetrachloride in hexanes; diethyl ether T=20°C; 3 h; Inert atmosphere;
参考文献
WO2011/136902 A1, ;
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