2-烯丙基-4-硝基苯酚合成路线 （共 14 条）
反应条件
1: 93 percent / K2CO3 / acetone / 2 h / 60 °C 2: 85 percent / [RuClH(CO)(PPh3)3] / CH2Cl2 / 14 h / 65 °C 3: 92 percent / ((Mes)2C3H5N2)Cl2Ru=CHPh / toluene / 3 h / 90 °C View Scheme
参考文献
Van Otterlo, Willem A.L.; Morgans, Garreth L.; Madeley, Lee G.; Kuzvidza, Samuel; Moleele, Simon S.; Thornton, Natalie; De Koning, Charles B.
Tetrahedron, 2005 , vol. 61, # 32 p. 7746 - 7755
反应条件
Rhodium trichloride; toluene-4-sulfonic acid in ethanol 5 h; Heating;
参考文献
Bujok, Robert; Bieniek, Michal; Masnyk, Marek; Michrowska, Anna; Sarosiek, Agata; Stepowska, Halszka; Arlt, Dieter; Grela, Karol
Journal of Organic Chemistry, 2004 , vol. 69, # 20 p. 6894 - 6896
反应条件
copper diacetate; lithium chloride; palladium dichloride in N,N-dimethyl-formamide T=100°C; 1.5 h; Yields of byproduct given;
参考文献
Roshchin, Alexander I.; Kel'chevski, Sergey M.; Bumagin, Nikolai A.
Journal of Organometallic Chemistry, 1998 , vol. 560, # 1-2 p. 163 - 167
反应条件
1: 96 percent / [RuClH(CO)(PPh3)3] / toluene / 24 h / 65 - 90 °C 2: 100 percent / K2CO3 / acetone / Heating 3: 100 percent / (1,3-dimesitylimidazolidin-2-yl)(PhCH=)RuCl2(PCy3) / toluene / 1 h / 60 °C View Scheme
参考文献
Van Otterlo, Willem A.L.; Ngidi, E. Lindani; Kuzvidza, Samuel; Morgans, Garreth L.; Moleele, Simon S.; De Koning, Charles B.
Tetrahedron, 2005 , vol. 61, # 42 p. 9996 - 10006
