反应条件
1: mCPBA / 1,2-dichloro-ethane / 0.25 h / 0 °C
2: 720 mg / toluene / 0.5 h / Heating
3: 95 percent / Dess-Martin periodinane / 1,2-dichloro-ethane / 0.25 h / 20 °C
4: 85 percent / CrCl2 / tetrahydrofuran / 8 h / 20 °C
5: 66 percent / Et3N; CuI / Pd(PPh3)4 / benzene; tetrahydrofuran / 2 h / 20 °C
6: H2 / Rh(PPh3)3Cl / benzene / 8 h
7: 1.0 mg / Me2S; BF3*Et2O / 0.08 h / 0 °C
View Scheme
参考文献
Makabe, Hidefumi; Tanaka, Akira; Oritani, Takayuki
Tetrahedron Letters, 1997 , vol. 38, # 24 p. 4247 - 4250
