T=120°C; 24 h; various ratio of reactants; also N-methylaniline, (3,3-dimethylallyl)diphenyl phosphate as reactants, corresponding products; Product distribution;

n-butyllithium; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; hexane under Ar, 1.6 M hexane soln. of n-BuLi added to suspn. of anhyd. SnCl2 in THF at 0°C, stirred for 20 min, treated with 1.0 M hexane soln. of Et2AlCl at 0°C, stirred for 20 min, mixt. of C3H5OPO(OPh)2 and P(PPh3)4 in THF, stirred for 1 h; poured into 5percent NaOH, extd. with ether, org. layer washed with 5percent NaOH, dried over anhyd. Na2SO4, concd., chromd. (Al2O3, hexane), distd. (bp 120°C (bath temp.)/0.1 Torr);

in N,N-dimethyl-formamide 3 h; Ambient temperature;

sodium iodide in N,N-dimethyl-formamide 3 h; Ambient temperature;

T=120°C; 24 h;

T=120°C; 24 h;

T=120°C; 24 h; various ratio of reactants; also N-methylaniline, (3,3-dimethylallyl)diphenyl phosphate as reactants, corresponding products; Product distribution;

lithium chloride in N,N-dimethyl-formamide 0.166667 h; Ambient temperature;

triphenylphosphine; Pd-Gr in tetrahydrofuran; water 0.5 h; Heating;

zinc; Co-complex 3 in N,N-dimethyl-formamide T=20°C;