反应条件
1: pyridine / 8 h / 0 °C
2: DIBAL-H / toluene / 7 h / -78 °C
3: dimethylaminopyridine / CH2Cl2 / 2 h / 0 °C
4: NaI / dimethylsulfoxide / 5 h / Ambient temperature
5: 100 percent / 5 mole percent Pd(PPh3)4, N(C2H5)3 / acetonitrile / 2 h / 70 °C
View Scheme
参考文献
Godleski, Stephen A.; Meinhart, James D.; Miller, David J.; Wallendael, Shawn Van
Tetrahedron Letters, 1981 , vol. 22, # 24 p. 2247 - 2250
