反应条件
<b>Multi-step reaction with 3 steps<br /> </b>1.1: 93 percent / KOH / ethanol; H<sub>2</sub>O / 2 h / 20 °C<br />2.1: 95 percent / H<sub>2</sub> / Pd/C / methanol / 2.5 h / 20 °C / 800 - 900 Torr<br />3.1: acetonitrile / Heating<br />3.2: Et<sub>3</sub>N; DMAP / CH<sub>2</sub>Cl<sub>2</sub> / 24 h / 20 °C<br />3.3: 57 mg / Alox B Super 1; MnO<sub>2</sub> / CH<sub>2</sub>Cl<sub>2</sub> / 0.75 h / 20 °C<br /> <br />
参考文献
Knoelker, Hans-Joachim; Froehner, Wolfgang; Reddy, Kethiri R. European Journal of Organic Chemistry, 2003 , # 4 p. 740 - 746
