三甲基-(1-苯乙烯基)硅烷合成路线 （共 49 条）
反应条件
NiCl2((PPh3)P)2 in toluene
16 h; Heating;
参考文献
Ni, Zhi-Jie; Yang, Pin-Fan; Ng, Dennis K. P.; Tzeng, Yih-Ling; Luh, Tien-Yau
Journal of the American Chemical Society, 1990 , vol. 112, # 25 p. 9356 - 9364
反应条件
potassium hydrogensulfate
T=150°C; P=10 Torr;
参考文献
Uchida, Tetsuro; Kita, Yoshio; Maekawa, Hirofumi; Nishiguchi, Ikuzo
Tetrahedron, 2006 , vol. 62, # 13 p. 3103 - 3111
反应条件
magnesium
T=170°C; 10 h;
参考文献
Voronkov, M. G.; Dubinskaya, E. I.; Putilova, G. G.; Larin, M. F.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 4 p. 678
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 4 p. 897
反应条件
bis(dibenzylideneacetone)-palladium(0) in acetonitrile
T=40°C; 2 h; Yield given. Yields of byproduct given;
参考文献
Ikenaga, Kazutoshi; Kikukawa, Kiyoshi; Matsuda, Tsutomu
Journal of Organic Chemistry, 1987 , vol. 52, # 7 p. 1276 - 1280
反应条件
in tetrahydrofuran
0.5 h; Ambient temperature;
参考文献
Fuerstner, Alois; Kollegger, Gerlinde; Weidmann, Hans
Journal of Organometallic Chemistry, 1991 , vol. 414, # 3 p. 295 - 305
反应条件
lithium diisopropyl amide in tetrahydrofuran
T=67°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Menichetti, Stefano; Stirling, Charles J. M.
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 13 p. 1511 - 1515
参考文献
Ikenaga, Kazutoshi; Matsumoto, Satoshi; Kikukawa, Kiyoshi; Matsuda, Tsutomu
Chemistry Letters, 1988 , # 5 p. 873 - 876
反应条件
in tetrahydrofuran
2 h; Ambient temperature;
参考文献
Fuerstner, Alois; Kollegger, Gerlinde; Weidmann, Hans
Journal of Organometallic Chemistry, 1991 , vol. 414, # 3 p. 295 - 305
反应条件
1: 74 percent / magnesium / dimethylformamide / 20 h / 20 °C
2: 66 percent / HCl / dimethylformamide; H2O / 8 h
3: 55 percent / anhydrous KHSO4 / 150 °C / 10 Torr
View Scheme
参考文献
Uchida, Tetsuro; Kita, Yoshio; Maekawa, Hirofumi; Nishiguchi, Ikuzo
Tetrahedron, 2006 , vol. 62, # 13 p. 3103 - 3111
反应条件
1: tetrahydrofuran / 3 h / 40 °C
2: H2O
View Scheme
参考文献
Vinod, Thottumkara K.; Hart, Harold
Tetrahedron Letters, 1988 , vol. 29, # 8 p. 885 - 888
