三甲基-(1-苯乙烯基)硅烷合成路线 (共 49 条)
反应条件
1: tetrahydrofuran / 3 h / 40 °C
2: H2O
View Scheme
参考文献
Vinod, Thottumkara K.; Hart, Harold
Tetrahedron Letters, 1988 , vol. 29, # 8 p. 885 - 888
反应条件
in tetrahydrofuran
0.5 h; Ambient temperature;
参考文献
Fuerstner, Alois; Kollegger, Gerlinde; Weidmann, Hans
Journal of Organometallic Chemistry, 1991 , vol. 414, # 3 p. 295 - 305
反应条件
lt;Bu4Ngt;lt;PtCl6gt;
T=80°C;
参考文献
E. Liepins; Goldberg, Yu.; Iovel, I.; Lukevics, E.
Journal of Organometallic Chemistry, 1987 , vol. 335, p. 301 - 312
反应条件
3-chloro-benzenecarboperoxoic acid
参考文献
Reich,H.J.; Shah,S.K.
Journal of Organic Chemistry, 1977 , vol. 42, # 10 p. 1773 - 1776
反应条件
1: (i) LDA, (ii) /BRN= 1209232/
2: (i) nBuLi, Et2NH, (ii) /BRN= 969135/
3: MCPBA
View Scheme
参考文献
Reich,H.J.; Shah,S.K.
Journal of Organic Chemistry, 1977 , vol. 42, # 10 p. 1773 - 1776
反应条件
1: (i) nBuLi, Et2NH, (ii) /BRN= 969135/
2: MCPBA
View Scheme
参考文献
Reich,H.J.; Shah,S.K.
Journal of Organic Chemistry, 1977 , vol. 42, # 10 p. 1773 - 1776
反应条件
1: (i) NaBH4, (ii) /BRN= 471308/
2: (i) LDA, (ii) /BRN= 1209232/
3: (i) nBuLi, Et2NH, (ii) /BRN= 969135/
4: MCPBA
View Scheme
参考文献
Reich,H.J.; Shah,S.K.
Journal of Organic Chemistry, 1977 , vol. 42, # 10 p. 1773 - 1776
参考文献
Cook,M.A. et al.
Journal of Organometallic Chemistry, 1971 , vol. 29, p. 389 - 396
反应条件
Li-naphthalenide
1) THF, 4 h, -78 deg C; 2) r.t.; Yield given. Multistep reaction;
参考文献
Ager, David J.
Journal of Organic Chemistry, 1984 , vol. 49, # 1 p. 168 - 170
反应条件
1: Mg
2: Mg
3: AcOH
View Scheme
参考文献
Dunogues,J. et al.
Journal of Organometallic Chemistry, 1975 , vol. 87, p. 169 - 181